第1个回答 2009-05-24
Take about 0.5 g, powder, buy 100 ml precision says the three-necked flask, join 25m1 methanol (4) solvent, chloroform, the heat water 1.5 hours, filtration, zhenggan methanol capacity to 5ml, shake, 0.45 muon m microfiltration membrane filtration, accordingly.
第2个回答 2009-05-24
Take about 0.5 g, powder, buy 100 ml precision says the three-necked flask, join 25m1 methanol (1:4) solvent, chloroform, the heat water 1.5 hours, filtration, zhenggan methanol capacity to 5ml, shake, 0.45 muon m microfiltration membrane filtration, accordingly.
第3个回答 2009-05-24
Medicinal powder from about 0.5g, said precision set,100ml flask, by adding 25m1 of methanol: chloroform (1:4) solvent, to return home heating in a water bath at 1.5 hours, filter, dry, methanol volume to 5ml , shake, 0.45μm millipore filtration, that is too.
第4个回答 2009-05-24
take the drug ingredient powder about 0.5g,weigh it precisely and then put it into round bottomed flask with a volume of 100ml,then add methanol and chloroform mixture(1:4) solvent into the flask and put it in the warm water.After heated 1.5 hours,filter the solution and evaporate to dryness.Then add methanol to make the volume of the solution precisely 5ml,shake it up.Use the microporous filtering film with pore size about 0.45μm to filter the solution,thus, the result comes out.
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第5个回答 2009-05-24
Take 0.5g powder of the medicinal material and weigh it precisely. Then put it into a flask with a round bottom and join in 25m1 methanol: chloroform solvent (1:4). After heating the flask in a liquid bath and reflowing the liquid for one hour and half, filter the liquid, steam it dry, dissolve to 5ml by methanol, shake it up and filter it using a membrane with 0.45μm micro holes. Finally it can be got.